2-Naphthoyl chloride → HCID 10083909, 화합물
반응식
[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH2:5].[CH:7]1[C:16]2[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=2)[CH:10]=[CH:9][C:8]=1[C:17](Cl)=[O:18]>N1C=CC=CC=1>[CH3:1][NH:2][C:3](=[S:6])[NH:4][NH:5][C:17]([C:8]1[CH:9]=[CH:10][C:11]2[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=2)[CH:7]=1)=[O:18]참가 물질
4
실험 절차
To a stirred room temperature solution of 4-methylthiosemicarbazide (5.91 g, 5.62×10-2 mole) and pyridine (150 ml) was added 2-naphthoyl chloride (10.7 g, 5.61×10-2 mole). After stirring overnight, the pyridine was evaporated at reduced pressure. The concentrate was treated with water and the undissolved product was collected by filtration and dried by suction.
후처리
- customthe pyridine was evaporated at reduced pressure
- additionThe concentrate was treated with water
- filtrationthe undissolved product was collected by filtration
- customdried by suction
출처 및 근거
- ORD 기록
- ord-c9281fd746634014bc2368dea7eb7761
- 출처 데이터셋
- uspto-grants-1990_02
- 특허 번호
- US04900743
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