Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
alpha-Hydroxytriazolam → 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | alpha-Hydroxytriazolam | HCID 1963 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate | HCID 70359440 | — |
반응 단계
In a manner similar to Example 12, a mixture of 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine and acetic anhydride was heated on the water bath to give 8-chloro-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine acetate (ester).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04902794 |
| 출처 데이터셋 | uspto-grants-1990_02 |
| ORD ID | ord-56f90f3cd8f44867a19c25169971f8bd |
| 출처 메모 | uspto-grants-1990_02 |