Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Valeric anhydride → 8-chloro-1-(hydroxymethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine valerate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Valeric anhydride | HCID 74959 | — |
| 반응물 | alpha-Hydroxyalprazolam | HCID 162244 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 8-chloro-1-(hydroxymethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine valerate | HCID 70359609 | — |
반응 단계
In a manner similar to Example 12, a mixture of 8-chloro-1-(hydroxymethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine and valeric anhydride were heated on the water bath to give 8-chloro-1-(hydroxymethyl)-6-phenyl-4H-s-triazolo[4,3-a][1,4]benzodiazepine valerate (ester).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04902794 |
| 출처 데이터셋 | uspto-grants-1990_02 |
| ORD ID | ord-711857131fcb46ac80ae9b83a691baed |
| 출처 메모 | uspto-grants-1990_02 |