Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propargyl alcohol → N-Boc-beta-alanine Propargyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propargyl alcohol | HCID 7859 | — |
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | N-((1,1-dimethylethoxy)carbonyl)-beta-alanine | HCID 76809 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | N-Boc-beta-alanine Propargyl Ester | HCID 11831152 | — |
반응 단계
N-Boc-β-alanine (1.91 g, 10.1 mmol) and propargyl alcohol (0.675 g, 12 mmol) were dissolved in EtOAc (25 mL). Dicyclohexyl-carbodiimide (DCC, 2.06 g, 10 mmol) was added to the solution and after 16 h of stirring at room temperature, the reaction mixture was filtered and evaporated to dryness under vacuum. Crude product yield
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07727713B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-71ffcbba883a4093b8e3933b35c16e12 |
| 출처 메모 | uspto-grants-2010_06 |