Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dicyclohexylcarbodiimide → Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 반응물 | 2-Aminoxy-acetic acid ethyl ester | HCID 19808 | — |
| 반응물 | 4-Pentynoic acid | HCID 22464 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Pent-4-ynoylaminooxy-acetic Acid Ethyl Ester | HCID 59336531 | — |
반응 단계
To a solution of 2-Aminoxy-acetic acid ethyl ester (573 mg, 4.8 mmol) and 4-Pentynoic acid (441 mg, 4.5 mmol) in 15 mL EtOAc were added dicyclohexylcarbodiimide (928 mg, 4.5 mmol) and the resulting mixture was stirred at room temperature for 16 h.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07727713B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-128be03e30fc479198b6496eaff8785b |
| 출처 메모 | uspto-grants-2010_06 |