Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol, 1-ethoxy-2,2,2-trifluoro- → 4-Trifluoromethyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol, 1-ethoxy-2,2,2-trifluoro- | HCID 9897 | — |
| 반응물 | 4-Trifluoromethyl-7-methyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 10270119 | — |
| 생성물 | 4-Trifluoromethyl-6-(2,2,2-trifluoroethyl)-6,7,8,9-tetrahydropyrido[2,3-g]quinolin-2(1H)-one | HCID 10154869 | — |
반응 단계
This compound was prepared in a similar fashion as that described in Example 84 from Compound 192 (Structure 33 of Scheme VI, where R1═H, n=1) and trifluoroacetaldehyde ethyl hemiacetal. 1H NMR (400 MHz, CDCl3) 11.32 (br. s, 1H), 7.11 (s, 1H), 7.02 (s, 1H), 6.99 (s, 1H), 3.88 (q, 2H, J=8.9), 3.47 (t, 2H, J=5.6), 2.93 (t, 2H, J=6.3), 2.03 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07727980B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-2a6bbf7ff0534d48a19790d0a4deee4c |
| 출처 메모 | uspto-grants-2010_06 |