참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2,3-Diaminotoluene | HCID 17593 | — |
| 반응물 | 6-Chloro-3-methoxypyridazine-4-carbaldehyde | HCID 84048811 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178494311 | HCID 178494311 | — |
반응 단계
6-Chloro-3-methoxypyridazine-4-carbaldehyde is dissolved in DMF, und 2,3-diaminotoluene is added. The reaction solution is heated at 120° C. in a microwave for 30 minutes. The crude product is purified on silica gel (eluent ethyl acetate in heptane). MS (ES+) m/z 275 (M+H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07727989B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-e986e39eba024f0d9b164fdcba6d54bc |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
