Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(3,5-Dimethoxyphenyl)methanamine → HCID 68583684, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (3,5-Dimethoxyphenyl)methanamine | HCID 420973 | — |
| 반응물 | 8-Cyclohexyl-2-methanesulfonyl-5-oxo-5,8-dihydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester | HCID 25223482 | — |
| 생성물 | HCID 68583684 | HCID 68583684 | — |
반응 단계
Using the procedure outlined in Example 28 Step F, the title compound was prepared from 3,5-dimethoxy-benzylamine and 8-cyclohexyl-2-methanesulfonyl-5-oxo-5,8-dihydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester (33 mg, 0.08 mmol). 8-Cyclohexyl-5-oxo-2-(3,5-dimethoxy-benzylamino)-5,8-dihydro-pyrido[2,3-d]pyrimidine-6-carboxylic acid ethyl ester was obtained as a white solid (29 mg, 90%). Mass Spectrum (LCMS, ESI pos.) Calcd. For C25H30N4O5: 467.22 (M+H). Found: 467.2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728003B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-0cd2521c5a3847ab8129827e4d8d4efa |
| 출처 메모 | uspto-grants-2010_06 |