참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | 4-Fluorophenethyl bromide | HCID 573153 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 4-Fluorophenethyltriphenylphosphonium bromide | HCID 22386745 | — |
반응 단계
4-Fluorophenylethyl bromide (700 mg, 3.44 mmol) was dissolved in toluene (4 mL), triphenylphosphine (904 mg, 3.44 mmol) added and the solution heated for 10 min in a sealed flask at 200° C. under microwave heating. After cooling to rt, the solvent was decanted and the title compound was obtained quantitatively as the remaining glassy solid, which was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07727999B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_06 |
|---|
| ORD ID | ord-ced818104f6646a0b4c67d321a5aa17e |
|---|
| 출처 메모 | uspto-grants-2010_06 |
|---|
