Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Anhydride → 1-Acetylindolin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Oxindole | HCID 321710 | — |
| 생성물 | 1-Acetylindolin-2-one | HCID 323719 | 93.7% |
반응 단계
Indoline-2-one (6.65 g, 50 mmol) and acetic anhydride (9 mL) were heated at reflux for 15 h. After cooling, the product was filtered and rinsed with Et2O to give 2a as solids after vacuum drying (8.2 g, yield: 93.7 %).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728008B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-a7734ec7f6ab472a91dc21117afbdc06 |
| 출처 메모 | uspto-grants-2010_06 |