참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Alpha-Aminobutyric Acid | HCID 6657 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2-(Acetylamino)butanoic acid | HCID 306107 | — |
반응 단계
163 g (1.58 mol) 2-aminobutanoic acid are dissolved in acetic acid, and 242 g (2.37 mol) acetic anhydride are added dropwise. The mixture is stirred for 2 h at 100° C. until completion of reaction, then the solution evaporated to dryness in vacuo. The solid residue is suspended in ethyl acetate, filtered and washed with diethyl ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07115602B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_10 |
|---|
| ORD ID | ord-1f439a35aca34f5790b48824d706b12d |
|---|
| 출처 메모 | uspto-grants-2006_10 |
|---|
