Dimethyl Sulfate → HCID 21936505, 화합물

HRID 1241686

반응식

HRID 1241686 반응식
[Cl:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([CH3:12])[CH:6]=[CH:5]2.[CH3:13][O:14][S:15]([O:18]C)(=[O:17])=[O:16]>>[CH3:13][O:14][S:15]([O-:18])(=[O:17])=[O:16].[CH3:13][N+:8]1[C:9]2[C:4](=[CH:3][C:2]([Cl:1])=[CH:11][CH:10]=2)[CH:5]=[CH:6][C:7]=1[CH3:12]

참가 물질

3

반응물 2

HCID 6497Dimethyl SulfateHCID 1359656-Chloroquinaldine2회

생성물 1

HCID 21936505HCID 21936505, 화합물수율 95%

실험 절차

6-Chloro-2-methyl quinoline, 3 (3 g, 16.9 mmol) was alkylated with dimethylsulphate (2.13 g, 16.9 mmol) as above to give the title compound (4.88 g, 16.1 mmol, 95%).

출처 및 근거

ORD 기록
ord-0daedcdce0d849f4b4874f0d84d7c772
출처 데이터셋
uspto-grants-2006_10
특허 번호
US07115619B2

연결된 노트

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