Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Disulfide → HCID 178507537, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | m-Aminobenzohydrazide | HCID 84178 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178507537 | HCID 178507537 | — |
반응 단계
3-Aminobenzhydrazide (5.76 g) was dissolved in ethanol (40 mL), and triethylamine (4.8 mL) and carbon disulfide (2.1 mL) were added to the solution. The mixture was heated under reflux for 4 hrs. The solvent was evaporated, and water was added. The precipitated solids were collected by filtration to give the title compound (5.06 g) as a pale-yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07115635B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-2272d54bcda141169e47c2ffb68a7bea |
| 출처 메모 | uspto-grants-2006_10 |