Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Methyl 2-(2-iodophenyl)acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | 2-Iodophenylacetic acid | HCID 2780090 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Methyl 2-(2-iodophenyl)acetate | HCID 640185 | 100% |
반응 단계
2-Iodophenylacetic acid (1.45 g) was added to a mixture of methanol (100 mL) and acetyl chloride (5 mL). After stirring at room temperature for 3 hours, the solvent was removed and the residue was dried under vacuum giving the desired 2-iodophenylacetic acid methyl ester. Yield=100%
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07115741B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-9648dbe8a0734f798b9e731b9c3a0a62 |
| 출처 메모 | uspto-grants-2006_10 |