Water → HCID 10955768, 화합물

HRID 1243958노트

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HRID 1243958 반응식
[C:1]([C:3]1[CH:17]=[CH:16][C:6]([O:7][C:8]2[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][CH:9]=2)=[CH:5][CH:4]=1)#[N:2].[OH2:18]>CS(O)(=O)=O>[CH3:15][O:14][C:11]1[CH:12]=[CH:13][C:8]([O:7][C:6]2[CH:16]=[CH:17][C:3]([C:1]([NH2:2])=[O:18])=[CH:4][CH:5]=2)=[CH:9][CH:10]=1

참가 물질

4

반응물 2

HCID 962WaterHCID 14902794-(4-methoxyphenoxy)benzonitrile

생성물 1

HCID 10955768HCID 10955768, 화합물

시약·촉매·용매 1

HCID 6395Methanesulfonic Acid용매

실험 절차

4-(4-Cyanophenoxy)-methoxybenzene (7.66 g, 34 mmol) and water (6.13 g, 340 mmol) in methanesulfonic acid (32.7 g) were heated to 80° C. for 16 hours. The cooled mixture was poured onto ice/water and after stirring for 1 hour the solid was collected and air dried yielding 8.4 g of 4-(4-methoxyphenoxy)benzamideas a white solid. GC-MS (m/z, EI): 243 [M]+.

후처리

  1. additionThe cooled mixture was poured onto ice/water
  2. customwas collected
  3. customair dried
  4. customyielding 8.4 g of 4-(4-methoxyphenoxy)benzamideas a white solid

출처 및 근거

ORD 기록
ord-fc5824291b5a4724bec697ce5ec4c850
출처 데이터셋
uspto-grants-2006_10
특허 번호
US07119201B2

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