참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | P-Chloroacetophenone | HCID 7467 | — |
| 반응물 | N,N,N-trimethyl-1,1-bis(1-methylethoxy)amine | HCID 87682 | — |
| 생성물 | (E)-1-(4-chlorophenyl)-3-(dimethylamino)prop-2-en-1-one | HCID 5375260 | — |
반응 단계
A solution of 1-(4-chlorophenyl)ethan-1-one (3.0 g, 19.3 mmol) and N,N, dimethylformamide diisopropylacetal (20 ml) was heated at 150° C. for 16 hours. The reaction mixture was cooled to 0° C. and treated with hexanes (20 ml). The resulting solid was collected via filtration and washed with hexanes to provide the title compound: EI-MS (m/z) 209 [M+1]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07122544B2 |
|---|
| 출처 데이터셋 | uspto-grants-2006_10 |
|---|
| ORD ID | ord-add7d44b36634cabbf222fc3fe0e6861 |
|---|
| 출처 메모 | uspto-grants-2006_10 |
|---|
