Methacrylic Acid → 2-Propenoic acid, 2-methyl-, trimethylsilyl ester
반응식
C(O[Si:5]([CH3:8])([CH3:7])[CH3:6])(=O)C.[C:9]([OH:14])(=[O:13])[C:10]([CH3:12])=[CH2:11]>CCCCCC>[C:9]([O:14][Si:5]([CH3:8])([CH3:7])[CH3:6])(=[O:13])[C:10]([CH3:12])=[CH2:11]참가 물질
4
실험 절차
20 ml of acetoxytrimethylsilane and 11.4 ml of commercial methacrylic acid (ATOFINA Norsocryl® MAA) in 100 ml of hexane are mixed and heated. Azeotropic distillation of acetic acid affords trimethylsilyl methacrylate.
후처리
- temperatureheated
- distillationAzeotropic distillation of acetic acid
출처 및 근거
- ORD 기록
- ord-84921c3b361f4ad9a245e308e86de751
- 출처 데이터셋
- uspto-grants-2006_10
- 특허 번호
- US07122692B2
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