Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Iodophenol → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Iodophenol | HCID 10784 | — |
| 반응물 | Phenylboronic acid pinacol ester | HCID 570673 | — |
| 생성물 | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734623 | — |
반응 단계
The above reaction procedure used for 2-iodophenol was followed. The reaction was faster, being complete before the first sample for gc analysis was withdrawn after 1 h 50 min reaction time. The amount of phenylboronic acid pinacol ester was higher than in the 2-iodophenol reaction (around 7%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07122694B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-23004de992854d06895bd83361499298 |
| 출처 메모 | uspto-grants-2006_10 |