Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → tert-Butyl (5,6-dimethyl-1H-benzimidazol-2-yl)methylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | tert-butyl N-(cyanomethyl)carbamate | HCID 545844 | — |
| 반응물 | 4,5-Diamino-ortho-xylene bishydrochloride | HCID 12210957 | — |
| 반응물 | HCID 178418582 | HCID 178418582 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | tert-Butyl (5,6-dimethyl-1H-benzimidazol-2-yl)methylcarbamate | HCID 86760280 | — |
반응 단계
1.3 g of a 30% NaOCH3 solution were added to tert-butyl cyanomethylcarbamate (0.4 g; 25.6 mmol) in 10 ml of CH3OH, and the mixture was stirred at room temperature for 1 h. After addition of 5.15 g of 4,5-diamino-ortho-xylene bishydrochloride, the reaction mixture was stirred overnight and then added to 100 ml of H2O, and the solid obtained by filtration was dried at 30° C. in vacuo. 0.5 g; ESI-MS [M+H+]=276
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07125883B1 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-d90121ed27e544c4a8893b6b9fd7a1be |
| 출처 메모 | uspto-grants-2006_10 |