Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → (3,5,5 Trimethyl hexyl) 4-aminobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Benzocaine | HCID 2337 | — |
| 반응물 | 3,5,5-Trimethyl-1-hexanol | HCID 18938 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 용매 | Cyclohexane | HCID 8078 | — |
| 생성물 | (3,5,5 Trimethyl hexyl) 4-aminobenzoate | HCID 69639835 | — |
반응 단계
Sodium metal (1 g cat.) was added to ethanol (30 mL) to give a solution which was added to a suspension of ethyl 4-aminobenzoate (175 g, 1.06 mol) and 3,5,5 trimethyl hexanol (200 g, 1.4 mol) in cyclohexane (300 mL). The suspension was heated under reflux for 24 hours with the azeotropic removal of ethanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07129204B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-74ff96502e7f4c339282b0b43bcc57c1 |
| 출처 메모 | uspto-grants-2006_10 |