3,4-Dichlorophenol → 2-(3,4-Dichlorophenoxy)-3-quinolinecarbaldehyde

반응식

[Cl:1][C:2]1[CH:3]=[C:4]([OH:9])[CH:5]=[CH:6][C:7]=1[Cl:8].Cl[C:11]1[C:20]([CH:21]=[O:22])=[CH:19][C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[N:12]=1>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:5]=[CH:6][C:7]=1[Cl:8])[O:9][C:11]1[C:20]([CH:21]=[O:22])=[CH:19][C:18]2[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=2)[N:12]=1

참가 물질

반응물 2

HCID 72583,4-Dichlorophenol

HCID 6909582-Chloro-3-quinolinecarboxaldehyde

생성물 1

HCID 219047082-(3,4-Dichlorophenoxy)-3-quinolinecarbaldehyde

실험 절차

The title compound was prepared according to preparation 65 starting from 3,4-dichlorophenol and 2-chloro-3-quinoline carboxaldehyde (Aldrich Chemical Co.); δH (CDCl3, 400 MHz) 7.19 (1H, m), 7.50 (3H, m), 7.74 (2H, m), 7.91 (1H, dd), 8.75 (1H, s), 10.59 (1H, s); MS rn/z318, 320 (MH+).

출처 및 근거

ORD 기록: ord-87d274cc00ba47f99f419eae37613869
출처 데이터셋: uspto-grants-2006_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07129234B2

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