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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1247008생성일: 2026년 10월 26일

Acetic Acid → Benzyl (S)-2-(7-amino-6-hydroxy-1H-indazol-1-yl)-1-methylethylcarbamate

https://huagongshe.com/reaction/1247008

반응식

참여 물질

역할이름HCID투입량
반응물Acetic AcidHCID 176—
반응물Benzyl (S)-2-(6-hydroxy-7-nitro-1H-indazol-1-yl)-1-methylethylcarbamateHCID 136335131—
촉매IronHCID 23925—
용매WaterHCID 962—
생성물Benzyl (S)-2-(7-amino-6-hydroxy-1H-indazol-1-yl)-1-methylethylcarbamateHCID 136335132—

반응 단계

The product from Step C (0.20 g, 0.54 mmol) was combined with acetic acid (5 mL), water (5 mL), and iron powder (0.30 g mmol) and stirred at room temperature for 1 h. The reaction mixture was filtered and evaporated to a dark oil (0.47 g) which was was used in the next reaction: LC/MS m/z 341.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07129257B1
출처 데이터셋uspto-grants-2006_10
ORD IDord-d1ba1fe31dfe4f2d875d8394fc094a6c
출처 메모uspto-grants-2006_10