Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
13-cis-Acitretin → Acitretin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 13-cis-Acitretin | HCID 6437841 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Acitretin | HCID 5284513 | 98.3% |
반응 단계
Crude acetretin (10 g) was added to acetone (300 ml) and stirred at 25–30° C. for 1 hour under nitrogen atmosphere. The suspension was then filtered, washed with acetone (100 ml) and dried under vacuum at 25–30° C. to obtain pure acitretin (8 g, Assay 98.3% by HPLC).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07129365B2 |
| 출처 데이터셋 | uspto-grants-2006_10 |
| ORD ID | ord-0a6a1dd62a144e049522c3ad6075d89a |
| 출처 메모 | uspto-grants-2006_10 |