3-Ethoxy-1-(3-pyridinyl)-2-propen-1-one → HCID 13475883, 화합물

HRID 1247953

반응식

HRID 1247953 반응식
C(O[CH:4]=[CH:5][C:6]([C:8]1[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=1)=O)C.[NH2:14][C:15]1[C:19]([C:20]([C:22]2[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=2)=[O:21])=[CH:18][NH:17][N:16]=1>C1(C)C(C)=CC=CC=1>[C:22]1([C:20]([C:19]2[CH:18]=[N:17][N:16]3[C:6]([C:8]4[CH:9]=[N:10][CH:11]=[CH:12][CH:13]=4)=[CH:5][CH:4]=[N:14][C:15]=23)=[O:21])[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

참가 물질

4

반응물 2

HCID 540323263-Ethoxy-1-(3-pyridinyl)-2-propen-1-oneHCID 178509267HCID 178509267, 화합물

생성물 1

HCID 13475883HCID 13475883, 화합물

시약·촉매·용매 1

HCID 7237O-Xylene용매

실험 절차

A mixture of 0.02 mole of 3-ethoxy-1-(3-pyridinyl)-2-propen-1-one, 0.02 mole of (3-amino-1H-pyrazol-4-yl)phenyl-methanone and 100 ml of xylene was refluxed for 12 hours. The solvent was removed and the residue dissolved in dichloromethane. This solution was dried over sodium sulfate and the product isolated as described in Example 1, as crystals, mp 202°-203° C.

후처리

  1. temperaturewas refluxed for 12 hours
  2. customThe solvent was removed
  3. dissolutionthe residue dissolved in dichloromethane
  4. dry with materialThis solution was dried over sodium sulfate
  5. customthe product isolated

출처 및 근거

ORD 기록
ord-c49638eb094243959a97d943725eda29
출처 데이터셋
uspto-grants-1985_06
특허 번호
US04521422

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