Acetone → N-[(4,6-Dimethoxy-1,3,5-triazin-2-yl)aminocarbonyl]-2-pyridinesulfonamide

반응식

[CH3:1][O:2][C:3]1[N:8]=[C:7]([O:9][CH3:10])[N:6]=[C:5]([NH:11][C:12](=S)[NH:13][S:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=2)(=[O:16])=[O:15])[N:4]=1.CC(C)=[O:26]>>[CH3:1][O:2][C:3]1[N:8]=[C:7]([O:9][CH3:10])[N:6]=[C:5]([NH:11][C:12]([NH:13][S:14]([C:17]2[CH:22]=[CH:21][CH:20]=[CH:19][N:18]=2)(=[O:16])=[O:15])=[O:26])[N:4]=1

참가 물질

반응물 2

HCID 180Acetone

HCID 20278358HCID 20278358, 화합물

생성물 1

HCID 20278363N-[(4,6-Dimethoxy-1,3,5-triazin-2-yl)aminocarbonyl]-2-pyridinesulfonamide

실험 절차

A mixture containing 2.7 g of N-[(4,6-dimethoxy-1,3,5-triazin-2-yl)aminothioxomethyl]-2-pyridinesulfonamide, 2.98 g of mercuric oxide and 75 ml of acetone is stirred at ambient temperature for 60 hours and then filtered. Evaporation of the filtrate in vacuo yields the desired product.

후처리

filtrationfiltered
customEvaporation of the filtrate in vacuo

출처 및 근거

ORD 기록: ord-b4ed3855addf497494da9a3705cc2100
출처 데이터셋: uspto-grants-1985_06
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04522645

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