Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Dichlorobenzoyl chloride → HCID 178496933, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Dichlorobenzoyl chloride | HCID 66645 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 반응물 | 5-Methoxybenzocyclobutene-1-carboxylic acid methyl ester | HCID 54118413 | — |
| 생성물 | HCID 178496933 | HCID 178496933 | — |
반응 단계
In a manner analogous to that described in Example 5, starting from 26.6 g of aluminium trichloride, 9.61 g of 5-methoxybenzocyclobutene-1-carboxylic acid methyl ester and 20.95 g of 2,4-dichlorobenzoyl chloride there is obtained 4-(2,4-dichlorobenzoyl)-5-hydroxybenzocyclobutene-1-carboxylic acid methyl ester having a melting point of 99°-100°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04523030 |
| 출처 데이터셋 | uspto-grants-1985_06 |
| ORD ID | ord-fbea0220bd6b49d5837f15bd072fe64a |
| 출처 메모 | uspto-grants-1985_06 |