Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → Glycine, N-cyclohexyl-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Glycine | HCID 750 | — |
| 반응물 | Cyclohexanone | HCID 7967 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Glycine, N-cyclohexyl- | HCID 42810 | — |
반응 단계
338 g of glycine (4.5 mols) is dissolved in 1.5 liters of deionized water. The solution is put into a 1-gallon autoclave. 25 g of 10% Pd on C, 551 g of cyclohexanone (5.6 mols) and 500 ml of ethanol are added. Hydrogenation is carried out at 60° C. between 56.2 and 70.3 kg/cm2. In the course of three hours a pressure drop corresponding to 98.4 kg/cm2 is observed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04525294 |
| 출처 데이터셋 | uspto-grants-1985_06 |
| ORD ID | ord-1c08be19be5049c8910ba5b48776a324 |
| 출처 메모 | uspto-grants-1985_06 |