Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Disulfide → HCID 13561953, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | Furfuryl Alcohol | HCID 7361 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-(Chloromethyl)furan | HCID 219520 | — |
| 반응물 | D-1,2,3,4-Tetrahydronorharman-3-carboxylic acid | HCID 675102 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 13561953 | HCID 13561953 | — |
반응 단계
In the same manner as descsribed in Example 32, (3R)-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (8.65 g), KOH (4.67 g), carbon disulfide (2.43 ml), 75% ethanol (120 ml) and furfuryl chloride which is prepared from furfuryl alcohol (9.24 g), thionyl chloride (12.34 g) and pyridine (8.94 g) are reacted and treated to give the title compound (2.31 g) as pale yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04628057 |
| 출처 데이터셋 | uspto-grants-1986_12 |
| ORD ID | ord-4d04b1f0650b4fee9de48418bb2f4bae |
| 출처 메모 | uspto-grants-1986_12 |