Potassium Carbonate → Quizalofop-methyl

HRID 1249112

반응식

HRID 1249112 반응식
Cl[C:2]1[CH:11]=[N:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([Cl:12])[CH:8]=2)[N:3]=1.[OH:13][C:14]1[CH:26]=[CH:25][C:17]([O:18][CH:19]([CH3:24])[C:20]([O:22][CH3:23])=[O:21])=[CH:16][CH:15]=1.C(=O)([O-])[O-].[K+].[K+]>C(#N)C>[Cl:12][C:7]1[CH:8]=[C:9]2[C:4](=[CH:5][CH:6]=1)[N:3]=[C:2]([O:13][C:14]1[CH:15]=[CH:16][C:17]([O:18][CH:19]([CH3:24])[C:20]([O:22][CH3:23])=[O:21])=[CH:25][CH:26]=1)[CH:11]=[N:10]2

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 877482,6-DichloroquinoxalineHCID 366926Propanoic acid, 2-(4-hydroxyphenoxy)-, methyl ester

생성물 1

HCID 187101Quizalofop-methyl

시약·촉매·용매 1

HCID 6342Acetonitrile용매

실험 절차

In 150 ml of acetonitrile, 2.0 g (0.01 mole) of 2,6-dichloroquinoxaline, 2.0 g (0.01 mole) of methyl 2-(4'-hydroxyphenoxy)propionate and 2.0 g (0.014 mole) of potassium carbonate were added and the mixture was refluxed for 24 hours.

후처리

  1. temperaturethe mixture was refluxed for 24 hours

출처 및 근거

ORD 기록
ord-066bb0bcec71408a9aff71d9cc731982
출처 데이터셋
uspto-grants-1986_12
특허 번호
US04629493

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