Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allylamine → 2-Allylamino-4-dodecylamino-6-nitroquinazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allylamine | HCID 7853 | — |
| 반응물 | 2-Chloro-4-dodecylamino-6-nitroquinazoline | HCID 18326516 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Allylamino-4-dodecylamino-6-nitroquinazoline | HCID 18326548 | 93.4% |
반응 단계
To 170 mg (0.44 mmol) of 2-chloro-4-dodecylamino-6-nitroquinazoline was added 1.70 ml (22.66 mmol) of allylamine, and then the resulting mixture was stirred at room temperature overnight. After water was added to the reaction solution, crystals thus precipitated were filtered to give 170 mg (93.4%) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06339089B2 |
| 출처 데이터셋 | uspto-grants-2002_01 |
| ORD ID | ord-46e3260cc7e241ce9c3303d32471a74b |
| 출처 메모 | uspto-grants-2002_01 |