참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Pulegol | HCID 92793 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | Neoisomenthol | HCID 19244 | 90% |
반응 단계
A 100 ml capacity autoclave was charged with 1.0 g (6.5 mmol) of pulegol, 5% Pd-carbon (20 mg) and ethyl acetate (5 ml), and the mixture was stirred at 60° C. for 5 hours under a hydrogen pressure of 2 Mpa. After completion of the reaction, the reaction solution was cooled to room temperature and concentrated. A 0.99 g portion of a mixture of menthol:neoisomenthol=91:9 was obtained. The yield was 90%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06342644B1 |
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| 출처 데이터셋 | uspto-grants-2002_01 |
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| ORD ID | ord-ee8680ab80ff49fab1bb95cf6419c2a8 |
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| 출처 메모 | uspto-grants-2002_01 |
|---|