Ethyl isothiocyanate → HCID 53787466, 화합물
반응식
[NH2:1][C:2]1[CH:6]=[N:5][N:4]([CH2:7][CH2:8][CH2:9][CH2:10][C:11]#[N:12])[N:3]=1.[CH2:13]([N:15]=[C:16]=[S:17])[CH3:14]>C(#N)C>[CH2:13]([NH:15][C:16](=[S:17])[NH:1][C:2]1[CH:6]=[N:5][N:4]([CH2:7][CH2:8][CH2:9][CH2:10][C:11]#[N:12])[N:3]=1)[CH3:14]참가 물질
4
실험 절차
A solution of 5-(4-amino-1,2,3-triazol-2-yl)valeronitrile (1.65 g.) in acetonitrile (6 ml.) was treated with ethylisothiocyanate (0.87 g.) and the solution stirred for 2.5 days then heated under reflux for 4.5 hours. Evaporation of the solvent gave 5-[4-(3-ethylthioureido)-1,2,3-triazol-2-yl]valeronitrile.
후처리
- temperaturethen heated
- temperatureunder reflux for 4.5 hours
- customEvaporation of the solvent
출처 및 근거
- ORD 기록
- ord-e82122b92bd14f68a638e6154bfec3c9
- 출처 데이터셋
- uspto-grants-1988_05
- 특허 번호
- US04748165
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