Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → Acetyltriphenylene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Triphenylene | HCID 9170 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Acetyltriphenylene | HCID 86641842 | 97% |
반응 단계
Triphenylene (1 equivalent) is reacted at 0° C. with 2.1 equivalents of AlCl3 and 21.0 equivalents of CH3COCl in CH2Cl2. After stirring at room temp. for 3 hours, the reaction product (acetyltriphenylene) was obtained in 97% yield, and is used in step b).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08455112B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-50762937bfe84de5b8de680d0acea52e |
| 출처 메모 | uspto-grants-2013_06 |