Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic acid, azido-, ethyl ester → Ethyl (2Z,4E)-2-azido-5-(4-methylphenyl)penta-2,4-dienoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic acid, azido-, ethyl ester | HCID 69480 | — |
| 반응물 | Sodium ethoxide | HCID 2723922 | — |
| 반응물 | p-Methylcinnamaldehyde | HCID 5371802 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Ethyl (2Z,4E)-2-azido-5-(4-methylphenyl)penta-2,4-dienoate | HCID 12378027 | — |
반응 단계
Following General Procedure I, a 1.38 M solution of NaOEt in ethanol (30 ml), (E)-3-(4-methylphenyl)acrylaldehyde (Compound 43, 1.1 g, 7.5 mmol) and ethyl azidoacetate (12 ml, 37.5 mmol) in EtOH (20 ml) were reacted to produce the title compound as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728014B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-b4766f87ad664e35965873e1b072eb02 |
| 출처 메모 | uspto-grants-2010_06 |