Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triphenylphosphine → 3-Ethoxycarbonyl-1,1,1-triphenyl-6-(4-methylphenyl)-2-aza-1lambda5-phosphahexa-1,3,5-triene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | Ethyl (2Z,4E)-2-azido-5-(4-methylphenyl)penta-2,4-dienoate | HCID 12378027 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-Ethoxycarbonyl-1,1,1-triphenyl-6-(4-methylphenyl)-2-aza-1lambda5-phosphahexa-1,3,5-triene | HCID 86761121 | — |
반응 단계
Following General Procedure J, triphenylphosphine (1.5 g, 5.8 mmol) ethyl (2Z,4E)-2-azido-5-(4-methylphenyl)penta-2,4-dienoate (Compound 45, 1.5 g, 5.8 mmol) in diethyl ether (50 ml) were reacted to produce the title compound as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728014B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-6b70e7d8fcb74f30a6fe09540ac7d36f |
| 출처 메모 | uspto-grants-2010_06 |