Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Pyridinecarboxaldehyde → Ethyl 3-(4-Ethylphenyl)-[2,4']-bipyridinyl-6-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Pyridinecarboxaldehyde | HCID 13389 | — |
| 반응물 | 3-Ethoxycarbonyl-1,1,1-triphenyl-6-(4-ethylphenyl)-2-aza-1lambda5-phosphahexa-1,3,5-triene | HCID 86619069 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Ethyl 3-(4-Ethylphenyl)-[2,4']-bipyridinyl-6-carboxylate | HCID 68408497 | — |
반응 단계
Following General Procedure K, 4-pyridinecarboxaldehyde (92 mg, 0.86 mmol) and 3-ethoxycarbonyl-1,1,1-triphenyl-6-(4-ethylphenyl)-2-aza-1λ5-phosphahexa-1,3,5-triene (Compound 46, 434 mg, 0.86 mmol) in dry acetonitrile (10 ml) were reacted to produce the title compound as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728014B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-785262fa1aa54b4eaa636014f7b15a5e |
| 출처 메모 | uspto-grants-2010_06 |