Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N'-Dimethylethylenediamine → 1-(5,6-Diphenyl-pyrazin-2-yl)-propan-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N'-Dimethylethylenediamine | HCID 8070 | — |
| 반응물 | Triethylaluminum | HCID 16682930 | — |
| 반응물 | Methyl 5,6-Diphenyl-pyrazine-2-carboxylate | HCID 25033170 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-(5,6-Diphenyl-pyrazin-2-yl)-propan-1-one | HCID 11231543 | — |
반응 단계
Following General Procedure O, methyl 5,6-diphenyl-pyrazine-2-carboxylate (Compound 93) (92 mg, 0.32 mmol), Et3Al (0.9 ml, 1M in hexane), DMEDA (38 mg, 0.35 mmol) in toluene was reacted to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07728014B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-c266ff78267141f78cd7efceb38cee8f |
| 출처 메모 | uspto-grants-2010_06 |