N-Ethylaniline → HCID 68508477, 화합물

HRID 1256900노트

반응식

HRID 1256900 반응식
[CH2:1]([N:3]([CH2:33][CH3:34])[C:4](=[O:32])[CH:5]([CH2:22][C:23]1[CH:28]=[CH:27][C:26]([N+:29]([O-:31])=[O:30])=[CH:25][CH:24]=1)[C:6]([NH:8][S:9]([C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=1)(=[O:11])=[O:10])=[O:7])[CH3:2].C(N[C:38]1[CH:43]=CC=[CH:40][CH:39]=1)C>>[CH2:33]([N:3]([C:1]1[CH:40]=[CH:39][CH:38]=[CH:43][CH:2]=1)[C:4](=[O:32])[CH:5]([CH2:22][C:23]1[CH:24]=[CH:25][C:26]([N+:29]([O-:31])=[O:30])=[CH:27][CH:28]=1)[C:6]([NH:8][S:9]([C:12]1[CH:21]=[CH:20][C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[CH:13]=1)(=[O:10])=[O:11])=[O:7])[CH3:34]

참가 물질

3

반응물 2

HCID 7670N-EthylanilineHCID 68506138HCID 68506138, 화합물

생성물 1

HCID 68508477HCID 68508477, 화합물수율 44%

실험 절차

In the same manner as in Example 1 (4), a crude product was obtained using the compound (500 mg) obtained in Example 6 (4) and N-ethylaniline (141 mg). This was purified by silica gel column chromatography to give the title compound (242 mg) as a white powder.

후처리

  1. customThis was purified by silica gel column chromatography

출처 및 근거

ORD 기록
ord-e3428e1a066546199abee791e57da91b
출처 데이터셋
uspto-grants-2013_06
특허 번호
US08461209B2

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