Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Oxalate → 3,4-Dihydroxy-thiophene-2,5-dicarboxylic acid diethyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Oxalate | HCID 7268 | — |
| 반응물 | Diethyl 2,2'-thiodiacetate | HCID 70216 | — |
| 생성물 | 3,4-Dihydroxy-thiophene-2,5-dicarboxylic acid diethyl ester | HCID 245503 | — |
반응 단계
The diethyl thioglycolate and diethyl oxalate are mixed, and then added to a first solution containing a first electron donor in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 100-500 W to perform a condensation reaction for 20-60 minutes to obtain 2,5-diethoxycarbonyl-3,4-dihydroxythiophene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08461355B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-143650d936db48c582b83b33620e8e81 |
| 출처 메모 | uspto-grants-2013_06 |