Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → 2,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Diethyl 2,3-dihydrothieno[3,4-b][1,4]dioxine-5,7-dicarboxylate | HCID 625399 | — |
| 생성물 | 2,3-Dihydro-thieno(3,4-b)(1,4)dioxin-5,7-dicarboxylic acid | HCID 728841 | — |
반응 단계
The 2,5-diethoxycarbonyl-3,4-ethylenedioxythiophene and NaOH are mixed in the microwave reactor. The microwave reactor is heated by the 2.45 GHz microwave at a power of 500-1200 W to perform hydrolysis reaction for no more than 20 minutes to obtain 2,5-dicarboxy-3,4-ethylenedioxythiophene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08461355B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-211382df869c46338f0100cc3b539058 |
| 출처 메모 | uspto-grants-2013_06 |