Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dilauryl Ether → 2-Methylundecane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dilauryl Ether | HCID 20667 | — |
| 반응물 | Trifluoromethanesulfonic acid | HCID 62406 | — |
| 반응물 | 10-Methyl-1-undecene | HCID 519941 | — |
| 반응물 | Isododecanol | HCID 6428591 | — |
| 생성물 | 2-Methylundecane | HCID 23459 | — |
반응 단계
300.0 g Lial® 123 (isododecanol from Sasol) and 18.0 g trifluoromethanesulfonic acid (50% by weight in water) were introduced into a distillation apparatus and heated for 1.5 h to 240° C. The organic phase of the distillate obtained (171.9 g) was dried over sodium sulfate and the product was isolated by filtration). The product then contained 91.5% isododecene, 7.5% Lial® 123 and 1.0% didodecyl ether (GC analysis).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08461407B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-48894196fe9f4034a9a0c2e7526108e1 |
| 출처 메모 | uspto-grants-2013_06 |