Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Thiophenesulfonamide → 2-Thiophenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Thiophenesulfonamide | HCID 72881 | — |
| 반응물 | (1,1'-Biphenyl)-4-sulphonyl chloride | HCID 74192 | — |
| 생성물 | 2-Thiophenesulfonamide | HCID 72881 | 90.6% |
| 생성물 | 4-Phenylbenzene-1-sulfonamide | HCID 5017140 | — |
반응 단계
4-biphenylsulfonamide was prepared according to the procedure for thiophene-2-sulfonamide YG1-030 except using 4-biphenylsulfonyl chloride, which afforded the title compound 642.2 mg (90.6%) as a white solid, m.p.: 223-225° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08466157B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-2ce01177aa1d41b18b3c319163567376 |
| 출처 메모 | uspto-grants-2013_06 |