Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Carbonate → 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-(Trifluoromethyl)piperidine | HCID 136469 | — |
| 반응물 | 4,5-Dichloro-n-methyl-2-nitroaniline | HCID 289317 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 4-Chloro-N-methyl-2-nitro-5-(4-trifluoromethyl-piperidin-1-yl)aniline | HCID 44120655 | — |
반응 단계
The sub-title compound was prepared from 4,5-dichloro-2-nitro-N-methyl-aniline (820 mg, 3.7 mmol), 4-trifluoromethyl-piperidine (680 mg, 4.5 mmol) and potassium carbonate (770 mg, 5.6 mmol) in DMSO (10 mL) in analogy to example 3, step (a).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08466186B2 |
| 출처 데이터셋 | uspto-grants-2013_06 |
| ORD ID | ord-9240ae367e324c91b9e6d9ef1785bbb1 |
| 출처 메모 | uspto-grants-2013_06 |