반응식
ClC1C(S)=C(Cl)C(Cl)=C(Cl)C=1Cl.[N+]([O-])(O)=O.[S:17](=[O:21])(=[O:20])([OH:19])[OH:18].[S:22](=[O:25])(=[O:24])=[O:23]>>[OH:20][S:17]([OH:21])(=[O:19])=[O:18].[O:23]=[S:22](=[O:25])=[O:24]참가 물질
5
실험 절차
reacting pentachlorothiophenol (PCTP) with a mixed nitration acid comprising nitric acid and sulfuric acid (and, preferably, sulfur trioxide to form oleum) at a temperature from about 35° to about 110° C. to form pentchloronitrobenzene, the nitric acid being in molar excess of the pentachlorothiophenol.
출처 및 근거
- ORD 기록
- ord-c754919d4a4f4e659eca6b7732cd2591
- 출처 데이터셋
- uspto-grants-1984_06
- 특허 번호
- US04454362
연결된 노트
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