Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → Methyl 4-formamidothiophene-3-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | Methyl 4-aminothiophene-3-carboxylate | HCID 2777610 | — |
| 반응물 | Sodium Acetate Trihydrate | HCID 23665404 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Methyl 4-formamidothiophene-3-carboxylate | HCID 2777637 | — |
반응 단계
A stirred solution of methyl 4-amino-3-thenoate (4 g), sodium acetate trihydrate (2.8 g) and formic acid (27 ml) was heated at 95° C. for 1 hour. On cooling the solution was poured into water, and the solution filtered to give the title product as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06541630B1 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-1f8a736f815c4486ba73f995478a54f7 |
| 출처 메모 | uspto-grants-2003_04 |