Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Diethyl Ether → Trichloromethylsilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Trichloromethylsilane | HCID 6399 | — |
| 반응물 | Chlorobenzene | HCID 7964 | — |
| 반응물 | Magnesium | HCID 5462224 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Trichloromethylsilane | HCID 6399 | — |
| 생성물 | Chloro(methyl)diphenylsilane | HCID 67349 | — |
반응 단계
The ether and phenylCl are fed in a ratio of 4:1 and the magnesium is fed at a rate to sustain the reaction as monitored by the reactor temperature profile, jacket water temperature rise, and agitator motor amps. The MeSiCl3 feed is varied to obtain a coupling ratio between 0.25 and 0.90 moles of PhCl/mole of MeSiCl3 depending on the ratio of Ph2SiMeCl/PhMeSiCl2 desired. Toluene is fed in at a 3:1 ratio to the PhenylCl in ether.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06541651B1 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-b4d890525b584637970382a80b33f372 |
| 출처 메모 | uspto-grants-2003_04 |