Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-Ethenyl-2-(iodomethyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Iodide | HCID 5238 | — |
| 반응물 | 1-(Chloromethyl)-2-ethenylbenzene | HCID 89757 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-Ethenyl-2-(iodomethyl)benzene | HCID 15830574 | 95% |
반응 단계
Dissolve 1-chloromethyl-2-vinyl-benzene (4.0 g, 26 mmol) in acetone (100 mL) and add sodium iodide (4.5 g, 30 mmol). Heat at gentle reflux for 30 minutes. Cool, add water (150 mL) and extract with pentane (200 mL). Dry (MgSO4) and evaporate the solvent in vacuo to give 1-iodomethyl-2-vinyl-benzene (95%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06544980B2 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-62360d8ce7814f55b21d359d07ada96b |
| 출처 메모 | uspto-grants-2003_04 |