Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-2',4'-difluoroacetophenone → HCID 18613919, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-2',4'-difluoroacetophenone | HCID 2774185 | — |
| 반응물 | Methyl 3-carbamothioylbenzoate | HCID 23279244 | — |
| 생성물 | HCID 18613919 | HCID 18613919 | 69% |
반응 단계
In the same manner as in Example 28, methyl 3-thiocarbamoylbenzoate was reacted with 2,4-difluorophenacyl bromide to obtain methyl 3-[4-(2,4-difluorophenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 69%. Pale yellow prisms. Melting point: 121 to 122° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06545009B1 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-5f0b24e3af384b42a4675a7710f40ee5 |
| 출처 메모 | uspto-grants-2003_04 |