Iron(2+) tetrafluoroborate--water (1/2/6) → Borate(1-), tetrafluoro-, iron(2+) (2:1)

반응식

O.O.O.O.O.O.[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]>ClCCl>[F:7][B-:8]([F:11])([F:10])[F:9].[F:12][B-:13]([F:16])([F:15])[F:14].[Fe+2:17]

참가 물질

실험 절차

To a suspension of iron(II) bis(tetrafluoroborate) hexahydrate (4.9 mg; 15 μmol) in dichloromethane was added a solution of h17 (5.0 mg; 14 μmol) in a few milliliters of dichloromethane. The solution turned from light yellow to dark orange with time within 18 hours. The solution was used as is in further polymerization study.

후처리

customwithin 18 hours

출처 및 근거

ORD 기록: ord-2e120f31d50341b7a2882bba00c0bdf9
출처 데이터셋: uspto-grants-2003_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06545108B1

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참가 물질

반응물 1

HCID 15762351Iron(2+) tetrafluoroborate--water (1/2/6)

생성물 1

HCID 11736352Borate(1-), tetrafluoro-, iron(2+) (2:1)

시약·촉매·용매 1

HCID 6344Dichloromethane용매2회

실험 절차

후처리

customwithin 18 hours

출처 및 근거

ORD 기록: ord-2e120f31d50341b7a2882bba00c0bdf9
출처 데이터셋: uspto-grants-2003_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06545108B1

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불러오는 중…