Perfluorooctanesulfonic acid → HCID 22726281, 화합물

HRID 1265963

반응식

HRID 1265963 반응식
[F:1][C:2]([F:29])([S:25]([OH:28])(=[O:27])=[O:26])[C:3]([F:24])([F:23])[C:4]([F:22])([F:21])[C:5]([F:20])([F:19])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].C(=O)([O-])[O-].[Ag+2:34]>O>[F:29][C:2]([F:1])([S:25]([O-:28])(=[O:27])=[O:26])[C:3]([F:23])([F:24])[C:4]([F:22])([F:21])[C:5]([F:19])([F:20])[C:6]([F:18])([F:17])[C:7]([F:16])([F:15])[C:8]([F:14])([F:13])[C:9]([F:12])([F:11])[F:10].[Ag+:34]

참가 물질

4

반응물 2

HCID 74483Perfluorooctanesulfonic acidHCID 178418647HCID 178418647, 화합물

생성물 1

HCID 22726281HCID 22726281, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

후처리

  1. additionwas added
  2. stirringAfter stirring at room temperature for 3 days
  3. filtrationthe mixture was filtered
  4. filtrationthe obtained filter-cake
  5. washwas washed with 10 parts of ion-exchange water
  6. dry with material20 parts of diethylether and dried

출처 및 근거

ORD 기록
ord-6ac8754eaec44102a8cb06ad7b0bca55
출처 데이터셋
uspto-grants-2003_04
특허 번호
US06548221B2

연결된 노트

불러오는 중…